Mortars
- Basic and applied research in the field of silicate technologies
- Design of optimal technologies in the field of mortars and burnt products
- Research and consultancy activities in the field of Portland clinker and cement quality
- Assessment and suitability testing of natural and secondary raw materials for clinker burning, cement production and other binding materials production, calculations of raw material meal composition
- Suitability assessment of limestone for lime burning and dolomites for half-burnt dolomite burning
- Suitability assessment of lime for lime hydrate production, possibilities of model tests
- Preparation and testing of autoclaved materials, prepared on basis of calcium hydro-silicates
- Suitability assessment of dolomites for industrial use
- Suitability verification of raw materials for the production of lightweight clay artificial aggregate and expanded perlite
Testing laboratory of mortars
- Verification and evaluation of the binding material quality according to standards CSN, EN and DIN and also according to customer´s methodology
- Determination of cement hydration heat by dissolving method according to Czech standard CSN EN 196-8
- Supplying of standards for calibration of Blaine apparatus used for specific surface determination
- Measurement of hydration temperatures course of hydraulic binders by means of differential and semi-adiabatic calorimeter
- Rheological properties testing of lime putty and other non-Newtonian fluids (Brookfield DV-E viscosimeter, Rheotest II. viscosimeter)
- Emley’s plasticity determination of lime putty (ASTM C110-76)
Adjustment
- Verification of physical-mechanical properties of raw materials from the point of adjustment process (determination of grindability according to Zeisel, VTI, abrasivity test etc.)
- Crushing, milling and homogenization of specimens up to 100 kg
- Sieve analyses on screening machine Alpine
- Firing in laboratory kilns up to 1700 °C and in amount up to 3 kg
- Flameproof finish of materials in model rotary kiln up to 1500 °C in amount 2 kg/h
Physical chemistry
X-ray diffractometric methods
Bruker D8 Advance diffractometer
- Qualitative phase analysis of inorganic materials (including indentification of asbestos minerals)
- Quantitative determination of crystalline and amorphous phases
- High-temperature X-ray diffractometry (identification of phase transformations up to 1600°C)
- Analysis of powder and solid samples
Optical methods
- Determination of quantitative phase composition of clinkers and cements by optical microscopy
- Slag glassiness determination, determination of slag and other admixtures content in cement
- Petrographical analyses of raw materials by means of optical microscopy
- Identification of alit and belit modifications in Portland cement clinker by high temperature microphotometry
- Fluorescence microscopy techniques
Thermic methods
Simultaneous thermal analyzer Perseus STA F3 Netzsch
- Simultaneous DTA/TG
- Simultaneous DSC/TG
- TG measurement
- Analysis of outgoing gases using FT-IR
- Maximal temperature ca. 1600 °C
- Heating speed up to 50 °C/min
- Measurement in controlled atmosphere (inert or oxidation)
- Qualitative and quantitative determination of some phases
Simultaneous thermal analyzer Netzsch STA 429
- Simultaneous DTA/TG
- TG measurement
- Maximal temperature ca. 1400 °C
- Heating speed up to 100 °C/min
- High-temperature dilatometry up to 1500 °C
- Determination of reactivity and burnability of raw material meal using kinetic method
Rheometric methods
Hybrid rheometer HR-1 Discovery (TA Instruments)
- Rheological properties determination of liquids, emulsions, dispersions, polymers, pastes, gels and also some solids
- Specifications – torque 10 nN.m – 150 mN.m, high resolution 10 nrad, angular velocity up to 300 rad/sec, normal force up to 50 N
- Measuring also with own geometries
- Regimes – oscillation measurement, flow measurement, creep regime
Other methods
- Porosity determination in range of 3,75 – 10000 nm by pressure mercury porosimetry
- Determination of specific surface by BET adsorption method
- Grading analysis of loose materials in range of 0,3 – 400 µm by means of laser grading analysis
- Determination of particles stability in dispersal environment using measurement of zeta potential and nanoparticle analysis (in range 2 – 3000 nm)
- Preparation of pure clinker phases (in kilograms)
Contact
Mgr. Martin Boháč, Ph.D.
mobile: +420 732 735 861
e-mail: bohac@vush.cz
Other related keywords
calorimetry, raw material composition, limestone, rheology, xonotlite, tobermorite, X-ray diffraction, rheometry |